Information card for entry 7058193

Structure parameters

• Formula: C33.25 H33.25 Cl0.75 F6 Fe N O P Pd Sb
• Calculated formula: C33 H33 F6 Fe N O P Pd Sb
• Title of publication: Synthesis and characterisation of palladium(ii) complexes with hybrid phosphinoferrocene ligands bearing additional O-donor substituents
• Authors of publication: Vosáhlo, Petr; Schulz, Jiří; Škoch, Karel; Císařová, Ivana; Štěpnička, Petr
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 11
• Pages of publication: 4463
• a: 10.5038 ± 0.0003 Å
• b: 16.8039 ± 0.0006 Å
• c: 22.1244 ± 0.0006 Å
• α: 68.4133 ± 0.0014°
• β: 79.3192 ± 0.001°
• γ: 71.842 ± 0.0011°
• Cell volume: 3439.28 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.0705
• Weighted residual factors for all reflections included in the refinement: 0.0753
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No