Information card for entry 7060674

Structure parameters

• Chemical name: LInCl2 (Mes)
• Formula: C34 H52 Cl2 In N3 P2
• Calculated formula: C34 H52 Cl2 In N3 P2
• Title of publication: Synthesis and characterization of group 13 dichloride (M = Ga, In), dimethyl (M = Al) and cationic methyl aluminum complexes supported by monoanionic NNN-pincer ligands
• Authors of publication: Chisholm, Desmond T.; Hayes, Paul G.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2021
• Journal volume: 45
• Journal issue: 33
• Pages of publication: 15043 - 15052
• a: 9.2843 ± 0.0001 Å
• b: 19.1068 ± 0.0003 Å
• c: 20.8295 ± 0.0003 Å
• α: 90°
• β: 92.334 ± 0.001°
• γ: 90°
• Cell volume: 3691.95 ± 0.09 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0369
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0875
• Weighted residual factors for all reflections included in the refinement: 0.0897
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No