Information card for entry 7061413

Structure parameters

• Formula: C39 H33 Cl N2 Pd
• Calculated formula: C39 H33 Cl N2 Pd
• Title of publication: A rigid-flexible double-layer steric strategy for ethylene (co)oligomerization with pyridine-imine Ni(ii) and Pd(ii) complexes
• Authors of publication: Yan, Zhengpeng; Bi, Huiqin; Ding, Beihang; Wang, Hui; Xu, Guoyong; Dai, Shengyu
• Journal of publication: New Journal of Chemistry
• Year of publication: 2022
• Journal volume: 46
• Journal issue: 18
• Pages of publication: 8669 - 8678
• a: 9.2957 ± 0.0009 Å
• b: 11.7588 ± 0.0011 Å
• c: 15.4097 ± 0.0014 Å
• α: 87.54 ± 0.003°
• β: 87.042 ± 0.003°
• γ: 70.733 ± 0.002°
• Cell volume: 1587.3 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0878
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1569
• Weighted residual factors for all reflections included in the refinement: 0.1671
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No