Information card for entry 7061797

Structure parameters

• Formula: C15 H27 Cl2 Cu N2 O P
• Calculated formula: C15 H27 Cl2 Cu N2 O P
• Title of publication: High-spin, tetrahedral cobalt(ii) and nickel(ii) complexes supported by monoprotic aminophosphine ligands, and attempted extension to copper(ii) complexes: synthesis, characterization, and unexpected reactivity
• Authors of publication: Kelly, Jordan C.; Bloomfield, Aaron J.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2022
• Journal volume: 46
• Journal issue: 39
• Pages of publication: 18647 - 18651
• a: 9.67 ± 0.004 Å
• b: 24.423 ± 0.009 Å
• c: 8.68 ± 0.003 Å
• α: 90°
• β: 102.684 ± 0.009°
• γ: 90°
• Cell volume: 1999.9 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0679
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0846
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No