Information card for entry 7063833

Structure parameters

• Formula: C48 H72 Cu6 N4 O26 Si10
• Calculated formula: C48 H72 Cu6 N4 O26 Si10
• Title of publication: Synthesis and structure of new vinylcoppersiloxanes and stereoregular organocyclosilsesquioxanes based on them
• Authors of publication: Frank, Inga V.; Shakirova, Albina R.; Peregudov, Alexander S.; Dolgushin, Fedor M.; Shchegolikhina, Olga I.; Anisimov, Anton A.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2025
• Journal volume: 49
• Journal issue: 26
• Pages of publication: 11273 - 11284
• a: 12.354 ± 0.0004 Å
• b: 14.1562 ± 0.0005 Å
• c: 20.9902 ± 0.0007 Å
• α: 90°
• β: 99.67 ± 0.001°
• γ: 90°
• Cell volume: 3618.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0682
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1372
• Weighted residual factors for all reflections included in the refinement: 0.1483
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No