Information card for entry 7101354

Structure parameters

• Common name: Compound 2
• Formula: C53 H42 B F25 P Rh
• Calculated formula: C53 H42 B F25 P Rh
• Title of publication: Phosphine-Olefin Ligands: A Facile Dehydrogenative Route to Catalytically Active Rhodium Complexes
• Authors of publication: Andrew Weller; Simon Brayshaw; Thomas M. Douglas; Christopher Frost; J.Le Notre
• Journal of publication: Chemical Communications
• Year of publication: 2006
• Journal issue: 32
• a: 19.5546 ± 0.0001 Å
• b: 16.3567 ± 0.0001 Å
• c: 34.5797 ± 0.0002 Å
• α: 90°
• β: 106.383 ± 0.0003°
• γ: 90°
• Cell volume: 10611.2 ± 0.11 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.06
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No