Metal cages using a bulky phosphonate as a ligand.
Authors of publication
Baskar, Viswanathan; Shanmugam, Muralidharan; Sañudo, E Carolina; Shanmugam, Maheswaran; Collison, David; McInnes, Eric J L; Wei, Qiang; Winpenny, Richard E P
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2007
Journal issue
1
Pages of publication
37 - 39
a
16.1648 ± 0.0011 Å
b
17.4547 ± 0.0015 Å
c
19.2761 ± 0.0013 Å
α
79.7 ± 0.006°
β
75.423 ± 0.006°
γ
69.81 ± 0.007°
Cell volume
4914.9 ± 0.6 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1938
Residual factor for significantly intense reflections
0.1021
Weighted residual factors for significantly intense reflections
0.241
Weighted residual factors for all reflections included in the refinement
0.2774
Goodness-of-fit parameter for all reflections included in the refinement
