Crystallography Open Database

Information card for entry 7101633

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Coordinates	7101633.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H173 Ge10 Li O4 Si19
Calculated formula	C64 H173 Ge10 Li O4 Si19
Title of publication	{Ge10Si[Si(SiMe3)3]4(SiMe32)Me}-: a Ge10Si framework reveals a structural transition onto elemental germanium.
Authors of publication	Schnepf, Andreas
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2006
Journal issue	2
Pages of publication	192 - 194
a	25.1875 ± 0.001 Å
b	19.9932 ± 0.0005 Å
c	47.964 ± 0.002 Å
α	90°
β	103.885 ± 0.003°
γ	90°
Cell volume	23447.9 ± 1.5 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0962
Residual factor for significantly intense reflections	0.0556
Weighted residual factors for significantly intense reflections	0.1285
Weighted residual factors for all reflections included in the refinement	0.1481
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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