Information card for entry 7101667
| Formula |
C69.5 H68 Cl2 O P4 Pd |
| Calculated formula |
C69.5 H56 Cl2 O P4 Pd |
| Title of publication |
Novel route to carbodiphosphoranes producing a new P,C,P pincer carbene ligand. |
| Authors of publication |
Stallinger, Silvia; Reitsamer, Christian; Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Peringer, Paul |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2007 |
| Journal issue |
5 |
| Pages of publication |
510 - 512 |
| a |
10.2001 ± 0.0002 Å |
| b |
12.4004 ± 0.0002 Å |
| c |
24.4161 ± 0.0004 Å |
| α |
84.068 ± 0.001° |
| β |
82.649 ± 0.001° |
| γ |
89.914 ± 0.001° |
| Cell volume |
3046.28 ± 0.09 Å3 |
| Cell temperature |
233 ± 2 K |
| Ambient diffraction temperature |
233 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0511 |
| Residual factor for significantly intense reflections |
0.0411 |
| Weighted residual factors for significantly intense reflections |
0.1042 |
| Weighted residual factors for all reflections included in the refinement |
0.1098 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.036 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/7101667.html
