Information card for entry 7101669

Structure parameters

• Formula: C56 H51.5 Cl6.5 P4
• Calculated formula: C56 H51.5 Cl6.5 P4
• Title of publication: Novel route to carbodiphosphoranes producing a new P,C,P pincer carbene ligand.
• Authors of publication: Stallinger, Silvia; Reitsamer, Christian; Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Peringer, Paul
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 5
• Pages of publication: 510 - 512
• a: 15.2377 ± 0.0006 Å
• b: 20.5124 ± 0.0007 Å
• c: 8.7621 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2738.7 ± 0.19 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 4
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1229
• Weighted residual factors for all reflections included in the refinement: 0.1283
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No