Information card for entry 7101912

Structure parameters

• Formula: C46 H68 N7 O Yb2
• Calculated formula: C46 H68 N7 O Yb2
• Title of publication: Synthesis and structural characterization of lanthanide complexes with the di- or tri-anionic diguanidinate ligand: new insight into the flexibility and distinct reactivity of the linked diguanidinate ligand.
• Authors of publication: Pi, Chengfu; Zhu, Zhenyu; Weng, Linhong; Chen, Zhenxia; Zhou, Xigeng
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 21
• Pages of publication: 2190 - 2192
• a: 18.734 ± 0.007 Å
• b: 9.805 ± 0.004 Å
• c: 26.843 ± 0.01 Å
• α: 90°
• β: 108.652 ± 0.005°
• γ: 90°
• Cell volume: 4672 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0582
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.0842
• Goodness-of-fit parameter for all reflections included in the refinement: 0.98
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No