Information card for entry 7102064

Structure parameters

• Common name: Bis(amidine)PdCl2 cyclohexane backbone
• Formula: C24 H24 Cl2 F6 N4 Pd
• Calculated formula: C24 H24 Cl2 F6 N4 Pd
• Title of publication: One-step assembly of a chiral palladium bis(acyclic diaminocarbene) complex and its unexpected oxidation to a bis(amidine) complex.
• Authors of publication: Wanniarachchi, Yoshitha A; Slaughter, LeGrande M
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 31
• Pages of publication: 3294 - 3296
• a: 12.8242 ± 0.0006 Å
• b: 24.6468 ± 0.0013 Å
• c: 8.0601 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2547.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0431
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0782
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No