Information card for entry 7102169

Structure parameters

• Formula: C67 H32 Ag9 Cl2 N O32 Os9 P2
• Calculated formula: C67 H32 Ag9 Cl2 N O32 Os9 P2
• SMILES: [Os]1234([Os]567([Os]81([Ag]19%10%113[Os]3%12%13([Ag]%14%15%16%17%18%19%10([Os]%10%20([Ag]%21689%14[Ag]68251[Os]1259([Ag]%14%22%113%156([Ag]3%16%10%2181([Ag]1682%14[Os]2%10%11([Os]%14%15%16([Os]12([Ag]%18%2038%15[Ag]%12%17%226%10%14)([O]%11%16)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])C5=O)C9=O)(C#[O])C#[O])(C#[O])(C#[O])(C%19=O)C#[O])C%13=O)(C#[O])(C#[O])C#[O])([O]47)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O].ClCCl.P(=N[P+](c1ccccc1)(c1ccccc1)c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Synthesis and characterisation of high-nuclearity osmium-silver mixed-metal clusters.
• Authors of publication: Lee, Yui-Bing; Wong, Wing-Tak
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 38
• Pages of publication: 3924 - 3926
• a: 14.587 ± 0.002 Å
• b: 18.744 ± 0.003 Å
• c: 19.042 ± 0.003 Å
• α: 63.828 ± 0.003°
• β: 69.54 ± 0.003°
• γ: 85.295 ± 0.003°
• Cell volume: 4361.8 ± 1.2 ų
• Cell temperature: 301 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0664
• Weighted residual factors for all reflections included in the refinement: 0.1019
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No