Information card for entry 7102173

Structure parameters

• Formula: C184 H122 Mo2 N8 O42 Si W12
• Calculated formula: C184 H120 Mo2 N8 O42 Si W12
• Title of publication: A discrete conglomerate of a distorted Mo(v)-porphyrin with a directly coordinated Keggin-type polyoxometalate.
• Authors of publication: Yokoyama, Atsutoshi; Kojima, Takahiko; Ohkubo, Kei; Fukuzumi, Shunichi
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 39
• Pages of publication: 3997 - 3999
• a: 18.4212 ± 0.0011 Å
• b: 37.5328 ± 0.0017 Å
• c: 17.8126 ± 0.0011 Å
• α: 90°
• β: 118.897 ± 0.002°
• γ: 90°
• Cell volume: 10782.2 ± 1 ų
• Cell temperature: 123.1 K
• Number of distinct elements: 7
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for significantly intense reflections: 0.0778
• Weighted residual factors for all reflections included in the refinement: 0.1817
• Goodness-of-fit parameter for all reflections included in the refinement: 1.2
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No