Information card for entry 7102284

Structure parameters

• Formula: C22 H51 Fe N3 P2 Si
• Calculated formula: C22 H51 Fe N3 P2 Si
• Title of publication: Transition metal dinitrogen complexes supported by a versatile monoanionic [N2P2] ligand.
• Authors of publication: Chomitz, Wayne A; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 45
• Pages of publication: 4797 - 4799
• a: 11.6476 ± 0.0011 Å
• b: 18.0559 ± 0.0018 Å
• c: 13.3821 ± 0.0013 Å
• α: 90°
• β: 102.055 ± 0.001°
• γ: 90°
• Cell volume: 2752.3 ± 0.5 ų
• Cell temperature: 154 ± 2 K
• Ambient diffraction temperature: 154 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.0936
• Goodness-of-fit parameter for all reflections included in the refinement: 1.576
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No