Information card for entry 7102335

Structure parameters

• Formula: C25 H56 B20 Cl3 O P3 Pt2
• Calculated formula: C25 H56 B20 Cl3 O P3 Pt2
• SMILES: ClC(Cl)Cl.[P]([Pt]123([P](C)(C)c4ccccc4)[BH]456[BH]789[BH]%1014[BH]1%11%127[Pt]7%13%14([P](C)(C)c4ccccc4)[BH]4%15%16[BH]%17%18%19[BH]%2074[BH]47%17[BH]%17%21%18[BH]%18%15%19[BH]%15%13%16[BH]%21%18([BH]%137%17[B]%14%204(O[B]42%10%11[BH]2%12([BH]781[BH]159[BH]527[BH]361[H]5)[H]4)[H]%13)[H]%15)(C)(C)c1ccccc1
• Title of publication: Macropolyhedral boron-containing cluster chemistry. Novel intercluster linkages from the reaction of [Pt(cod)Cl2] and [PtMe2(PMe2Ph)2] with 6,6'-(B10H13)2O.
• Authors of publication: Bould, Jonathan; Kennedy, John D
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 47
• Pages of publication: 5084 - 5086
• a: 10.6336 ± 0.0002 Å
• b: 14.8948 ± 0.0002 Å
• c: 15.7371 ± 0.0002 Å
• α: 66.761 ± 0.001°
• β: 83.475 ± 0.002°
• γ: 86.483 ± 0.002°
• Cell volume: 2275.09 ± 0.06 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1355
• Weighted residual factors for all reflections included in the refinement: 0.1428
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No