Information card for entry 7102337

Structure parameters

• Formula: C22 H40 Cu3 I3 N P5
• Calculated formula: C22 H40 Cu3 I3 N P5
• Title of publication: Copper(I) mediated oligomerisation of a phosphaalkyne.
• Authors of publication: Vogel, Ulf; Nixon, John F; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 47
• Pages of publication: 5055 - 5057
• a: 11.693 ± 0.002 Å
• b: 12.8918 ± 0.0016 Å
• c: 13.172 ± 0.003 Å
• α: 89.985 ± 0.013°
• β: 64.793 ± 0.018°
• γ: 77.478 ± 0.012°
• Cell volume: 1744.2 ± 0.6 ų
• Cell temperature: 103 ± 1 K
• Ambient diffraction temperature: 103 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0749
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0628
• Weighted residual factors for all reflections included in the refinement: 0.0655
• Goodness-of-fit parameter for all reflections included in the refinement: 0.811
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: cukα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No