Information card for entry 7102377

Structure parameters

• Formula: C44 H44 Cu4 F24 N12 P4
• Calculated formula: C44 H44 Cu4 F24 N12 P4
• Title of publication: Bowl-shaped Cu(I) metallamacrocyclic ethylene and carbonyl adducts as structural analogues of organic calixarenes.
• Authors of publication: Maekawa, Masahiko; Konaka, Hisashi; Minematsu, Toshie; Kuroda-Sowa, Takayoshi; Munakata, Megumu; Kitagawa, Susumu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 48
• Pages of publication: 5179 - 5181
• a: 14.6057 ± 0.0009 Å
• b: 28.37 ± 0.002 Å
• c: 14.0685 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5829 ± 1 ų
• Cell temperature: 150.2 K
• Number of distinct elements: 6
• Space group number: 45
• Hermann-Mauguin space group symbol: I b a 2
• Hall space group symbol: I 2 -2c
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for all reflections included in the refinement: 0.0964
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No