Information card for entry 7102407

Structure parameters

• Formula: C24 H32 F8 P2 Pd
• Calculated formula: C24 H30 F8 P2 Pd
• Title of publication: Synthesis and structural characterization of the first unsymmetrical diarylpalladium complex trans-Pd(C6F5)(2,4,6-C6F3H2)(PEt3)2, derived from transmetallation between 2,4,6-trifluorophenylboronic acid and trans-Pd(C6F5)I(PEt3)2.
• Authors of publication: Nishihara, Yasushi; Onodera, Hiroyuki; Osakada, Kohtaro
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 2
• Pages of publication: 192 - 193
• a: 12.309 ± 0.004 Å
• b: 12.207 ± 0.005 Å
• c: 9.46 ± 0.003 Å
• α: 90°
• β: 104.81 ± 0.03°
• γ: 90°
• Cell volume: 1374.2 ± 0.8 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for all reflections: 0.037
• Weighted residual factors for all reflections included in the refinement: 0.037
• Goodness-of-fit parameter for all reflections: 2.024
• Goodness-of-fit parameter for all reflections included in the refinement: 2.02
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No