Information card for entry 7102696

Structure parameters

• Formula: C4 F12 N2 O8 S4 Zn
• Calculated formula: C4 F12 N2 O8 S4 Zn
• Title of publication: Metal bis[trifluoromethyl)sulfonyl]amide complexes: highly efficient Friedel-Crafts acylation catalysts.
• Authors of publication: Earle, Martyn J; Hakala, Ullastiina; McAuley, Barry J; Nieuwenhuyzen, Mark; Ramani, Alwar; Seddon, Kenneth R
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 12
• Pages of publication: 1368 - 1369
• a: 11.556 ± 0.006 Å
• b: 5.16 ± 0.002 Å
• c: 14.189 ± 0.007 Å
• α: 90°
• β: 100.753 ± 0.01°
• γ: 90°
• Cell volume: 831.1 ± 0.7 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1306
• Residual factor for significantly intense reflections: 0.0664
• Weighted residual factors for significantly intense reflections: 0.1515
• Weighted residual factors for all reflections included in the refinement: 0.1892
• Goodness-of-fit parameter for all reflections included in the refinement: 0.939
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No