Information card for entry 7102698

Structure parameters

• Formula: C106 H126 Ni10 O31
• Calculated formula: C106 H128 Ni10 O31
• Title of publication: Supertetrahedral decametallic Ni(II) clusters directed by micro(6)-tris-alkoxides.
• Authors of publication: Shaw, Rachel; Tidmarsh, Ian S; Laye, Rebecca H; Breeze, Barbara; Helliwell, Madeleine; Brechin, Euan K; Heath, Sarah L; Murrie, Mark; Ochsenbein, Stefan; Gudel, Hans-Ulrich; McInnes, Eric J L
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 12
• Pages of publication: 1418 - 1419
• a: 24.723 ± 0.002 Å
• b: 24.201 ± 0.002 Å
• c: 17.649 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10559.6 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.1416
• Weighted residual factors for all reflections included in the refinement: 0.1576
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No