Information card for entry 7102729

Structure parameters

• Formula: C36 H24 F12 N6 Os P2
• Calculated formula: C36 H24 F12 N6 Os P2
• Title of publication: Formation of racemic crystals of transition metal complexes by grinding 1 : 1 mixtures of enantiomeric crystals.
• Authors of publication: Nakamura, Asao; Sato, Tomohiro; Kuroda, Reiko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 24
• Pages of publication: 2858 - 2859
• a: 36.943 ± 0.004 Å
• b: 16.1178 ± 0.0015 Å
• c: 12.1037 ± 0.0011 Å
• α: 90°
• β: 100.993 ± 0.002°
• γ: 90°
• Cell volume: 7074.7 ± 1.1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0385
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0764
• Weighted residual factors for all reflections included in the refinement: 0.0793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No