Information card for entry 7102755

Structure parameters

• Formula: C17 H19 B N6 O2 Si W
• Calculated formula: C17 H19 B N6 O2 Si W
• Title of publication: A mercury bis(tricarbido) complex: [Hg{C triple bond C-C triple bond W(CO)2Tp}2(dmso)4](dmso)2 (Tp = hydrotrispyrazolylborate).
• Authors of publication: Dewhurst, Rian D; Hill, Anthony F; Willis, Anthony C
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 24
• Pages of publication: 2826 - 2827
• a: 38.1017 ± 0.0005 Å
• b: 38.1017 ± 0.0005 Å
• c: 8.1896 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 10296.3 ± 0.2 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.0269
• Weighted residual factors for all reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0282
• Weighted residual factors for all reflections included in the refinement: 0.0282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1247
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No