Information card for entry 7102801

Structure parameters

• Formula: C26 H68 N5 Na Si2 Zn
• Calculated formula: C26 H68 N5 Na Si2 Zn
• SMILES: C(C)(C)(C)[Zn](C(C)(C)C)N([Si](C)(C)C)[Si](C)(C)C.[N]1(CC[N](C)(C)[Na]12[N](CC[N]2(C)C)(C)C)(C)C
• Title of publication: Transamination chemistry of sodium TMP-zincate: synthesis and crystal structure of a chiral amidozincate
• Authors of publication: Armstrong, David R.; Clegg, William; Dale, Sophie H.; García-Álvarez, Joaquín; Harrington, Ross W.; Hevia, Eva; Honeyman, Gordon W.; Kennedy, Alan R.; Mulvey, Robert E.; O'Hara, Charles T.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2008
• Journal issue: 2
• Pages of publication: 187 - 189
• a: 9.3269 ± 0.0012 Å
• b: 10.649 ± 0.002 Å
• c: 19.8598 ± 0.0012 Å
• α: 81.74 ± 0.01°
• β: 78.079 ± 0.01°
• γ: 83.872 ± 0.012°
• Cell volume: 1904 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0696
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0792
• Weighted residual factors for all reflections included in the refinement: 0.0907
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No