Information card for entry 7102885

Structure parameters

• Formula: C153 H122 Cl14 Cu4 N4 P4
• Calculated formula: C153 H122 Cl14 Cu4 N4 P4
• Title of publication: Stereoselective coordination of ditopic phospholyl-azahelicenes: a novel approach towards structural diversity in chiral pi-conjugated assemblies.
• Authors of publication: Shen, Wenting; Graule, Sébastien; Crassous, Jeanne; Lescop, Christophe; Gornitzka, Heinz; Réau, Régis
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 7
• Pages of publication: 850 - 852
• a: 32.938 ± 0.002 Å
• b: 19.965 ± 0.001 Å
• c: 24.449 ± 0.001 Å
• α: 90°
• β: 124.683 ± 0.002°
• γ: 90°
• Cell volume: 13221 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1187
• Weighted residual factors for all reflections included in the refinement: 0.1302
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No