Information card for entry 7102902

Structure parameters

• Formula: C48 H96 Li3 O24 Sb11
• Calculated formula: C48 H96 Li3 O24 Sb11
• Title of publication: Direct synthesis of the 1,2,3-[C6H4P...P...P]- anion, isoelectronic with the indenyl anion [C6H4CH...CH...CH]-.
• Authors of publication: García, Felipe; Less, Robert J; Naseri, Vesal; McPartlin, Mary; Rawson, Jeremy M; Sancho Tomas, Maria; Wright, Dominic S
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 7
• Pages of publication: 859 - 861
• a: 21.138 ± 0.002 Å
• b: 21.138 ± 0.002 Å
• c: 32.33 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 12510.2 ± 1.8 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.0984
• Residual factor for significantly intense reflections: 0.0721
• Weighted residual factors for significantly intense reflections: 0.1768
• Weighted residual factors for all reflections included in the refinement: 0.1975
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No