Information card for entry 7102975

Structure parameters

• Formula: C72 H107 O44 Rb5
• Calculated formula: C72 H56 O43.99 Rb5
• Title of publication: Interpenetrated nano-capsule networks based on the alkali metal assisted assembly of p-carboxylatocalix[4]arene-O-methyl ether.
• Authors of publication: Dalgarno, Scott J; Claudio-Bosque, Karla M; Warren, John E; Glass, Timothy E; Atwood, Jerry L
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 12
• Pages of publication: 1410 - 1412
• a: 28.0956 ± 0.0003 Å
• b: 28.0956 ± 0.0003 Å
• c: 64.0922 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 43813.9 ± 1.1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 161
• Hermann-Mauguin space group symbol: R 3 c :H
• Hall space group symbol: R 3 -2"c
• Residual factor for all reflections: 0.1456
• Residual factor for significantly intense reflections: 0.1202
• Weighted residual factors for significantly intense reflections: 0.3086
• Weighted residual factors for all reflections included in the refinement: 0.328
• Goodness-of-fit parameter for all reflections included in the refinement: 2.073
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.671 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No