Information card for entry 7103039

Structure parameters

• Formula: H168 K3 Li5.5 Na10 Ni3.75 O235 P6 W41
• Calculated formula: K3 Li2 Na10 Ni3.75 O187 P6 W41
• Title of publication: New trimeric polyoxotungstate aggregates based on [P2W12O48]14- building blocks.
• Authors of publication: Zhang, Zhi-Ming; Yao, Shuang; Li, Yang-Guang; Wang, Yong-Hui; Qi, Yan-Fei; Wang, En-Bo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 14
• Pages of publication: 1650 - 1652
• a: 19.187 ± 0.004 Å
• b: 20.947 ± 0.004 Å
• c: 28.482 ± 0.006 Å
• α: 75.34 ± 0.03°
• β: 79.86 ± 0.03°
• γ: 73.54 ± 0.03°
• Cell volume: 10553 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1589
• Residual factor for significantly intense reflections: 0.0759
• Weighted residual factors for significantly intense reflections: 0.163
• Weighted residual factors for all reflections included in the refinement: 0.1982
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No