Information card for entry 7103144

Structure parameters

• Formula: C66 H92 F6 O3 P Pd S3 Sb
• Calculated formula: C66 H92 F6 O3 P Pd S3 Sb
• Title of publication: Anion complexation via C-H...X interactions using a palladacyclic receptor.
• Authors of publication: Bedford, Robin B; Betham, Michael; Butts, Craig P; Coles, Simon J; Hursthouse, Michael B; Noelle Scully, P; Tucker, James H R; Wilkie, John; Willener, Yasmine
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 21
• Pages of publication: 2429 - 2431
• a: 12.32 ± 0.02 Å
• b: 12.719 ± 0.013 Å
• c: 22.1 ± 0.05 Å
• α: 83.91 ± 0.11°
• β: 79.8 ± 0.2°
• γ: 78.56 ± 0.08°
• Cell volume: 3332 ± 10 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1164
• Residual factor for significantly intense reflections: 0.0757
• Weighted residual factors for significantly intense reflections: 0.1701
• Weighted residual factors for all reflections included in the refinement: 0.1868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No