Information card for entry 7103211

Structure parameters

• Formula: C36 H74 K2 O4 Si4
• Calculated formula: C36 H74 K2 O4 Si4
• Title of publication: s-Block metal complexes of a bulky, donor-functionalized allyl ligand.
• Authors of publication: Solomon, Sophia A; Muryn, Christopher A; Layfield, Richard A
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 27
• Pages of publication: 3142 - 3144
• a: 10.9205 ± 0.0018 Å
• b: 18.729 ± 0.003 Å
• c: 11.286 ± 0.0018 Å
• α: 90°
• β: 97.988 ± 0.003°
• γ: 90°
• Cell volume: 2285.9 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No