Crystallography Open Database

Information card for entry 7103244

Preview

Coordinates	7103244.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H16 N4 O9 Pb2
Calculated formula	C19 H16 N4 O9 Pb2
Title of publication	Crystal-to-crystal transformation from a chain polymer to a two-dimensional network by thermal desolvation.
Authors of publication	Aslani, Alireza; Morsali, Ali
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2008
Journal issue	29
Pages of publication	3402 - 3404
a	10.403 ± 0.001 Å
b	10.719 ± 0.001 Å
c	11.372 ± 0.001 Å
α	69.8 ± 0.05°
β	87.18 ± 0.05°
γ	67.07 ± 0.05°
Cell volume	1090.7 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0371
Weighted residual factors for significantly intense reflections	0.0983
Weighted residual factors for all reflections included in the refinement	0.105
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7103244.html