Information card for entry 7103275

Structure parameters

• Common name: Pd-complex
• Chemical name: Pd-complex
• Formula: C22 H22 Cl2 N2 O4 Pd
• Calculated formula: C22 H22 Cl2 N2 O4 Pd
• Title of publication: Catalytic aerobic oxidation of substituted 8-methylquinolines in Pd(II)-2,6-pyridinedicarboxylic acid systems.
• Authors of publication: Zhang, Jing; Khaskin, Eugene; Anderson, Nicholas P; Zavalij, Peter Y; Vedernikov, Andrei N
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 31
• Pages of publication: 3625 - 3627
• a: 9.853 ± 0.0003 Å
• b: 10.5424 ± 0.0003 Å
• c: 10.9053 ± 0.0003 Å
• α: 95.7794 ± 0.0004°
• β: 96.0116 ± 0.0004°
• γ: 100.745 ± 0.0004°
• Cell volume: 1098.39 ± 0.05 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.027
• Residual factor for significantly intense reflections: 0.024
• Weighted residual factors for significantly intense reflections: 0.0514
• Weighted residual factors for all reflections included in the refinement: 0.0523
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No