Information card for entry 7103508

Structure parameters

• Formula: C22 H24 N2 O20 Zn5
• Calculated formula: C22 H24 N2 O20 Zn5
• Title of publication: Chemoenzymatic synthesis of chiral 4,4'-bipyridyls and their metal-organic frameworks.
• Authors of publication: Sbircea, Lenuta; Sharma, Narain D; Clegg, William; Harrington, Ross W; Horton, Peter N; Hursthouse, Michael B; Apperley, David C; Boyd, Derek R; James, Stuart L
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 43
• Pages of publication: 5538 - 5540
• a: 9.1586 ± 0.0004 Å
• b: 9.7969 ± 0.0004 Å
• c: 9.873 ± 0.0005 Å
• α: 77.598 ± 0.002°
• β: 89.947 ± 0.003°
• γ: 88.06 ± 0.003°
• Cell volume: 864.68 ± 0.07 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1281
• Weighted residual factors for all reflections included in the refinement: 0.1346
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No