Information card for entry 7103548

Structure parameters

• Formula: C62 H91 Fe N2
• Calculated formula: C62 H91 Fe N2
• Title of publication: Reaction of a sterically encumbered iron(I) aryl/arene with organoazides: formation of an iron(V) bis(imide).
• Authors of publication: Ni, Chengbao; Fettinger, James C; Long, Gary J; Brynda, Marcin; Power, Philip P
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 45
• Pages of publication: 6045 - 6047
• a: 13.9437 ± 0.0014 Å
• b: 14.9787 ± 0.0015 Å
• c: 15.5738 ± 0.0016 Å
• α: 82.3806 ± 0.0015°
• β: 66.0829 ± 0.0014°
• γ: 65.8148 ± 0.0014°
• Cell volume: 2710.2 ± 0.5 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0556
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.1047
• Weighted residual factors for all reflections included in the refinement: 0.115
• Goodness-of-fit parameter for all reflections included in the refinement: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No