Information card for entry 7103608

Structure parameters

• Common name: diazomethylstannylene
• Formula: C40 H58 N2 Si Sn
• Calculated formula: C40 H58 N2 Si Sn
• Title of publication: Formation of a stannylstannylene via intramolecular carbene addition of a transient stannaacetylene (RSn[triple bond, length as m-dash]CR').
• Authors of publication: Setaka, Wataru; Hirai, Katsuyuki; Tomioka, Hideo; Sakamoto, Kenkichi; Kira, Mitsuo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 48
• Pages of publication: 6558 - 6560
• a: 10.155 ± 0.003 Å
• b: 10.299 ± 0.003 Å
• c: 21.771 ± 0.006 Å
• α: 83.444 ± 0.005°
• β: 82.344 ± 0.006°
• γ: 62.356 ± 0.005°
• Cell volume: 1995.5 ± 1 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0985
• Residual factor for significantly intense reflections: 0.0766
• Weighted residual factors for significantly intense reflections: 0.1953
• Weighted residual factors for all reflections included in the refinement: 0.2056
• Goodness-of-fit parameter for all reflections included in the refinement: 1.141
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No