Pinwheel motifs: formation of unusual homo- and hetero-nuclear aggregates via bridging thiolates
Authors of publication
Amoroso, Angelo J.; Chung, Simon S. M.; Spencer, Douglas J. E.; Danks, Jonathan P.; Glenny, Mark W.; Blake, Alexander J.; Cooke, Paul A.; Wilson, Claire; Schröder, Martin
Journal of publication
Chemical Communications (Cambridge, United Kingdom)
Year of publication
2003
Journal issue
16
Pages of publication
2020 - 2021
a
11.594 ± 0.005 Å
b
13.393 ± 0.006 Å
c
25.598 ± 0.011 Å
α
77.182 ± 0.007°
β
89.969 ± 0.008°
γ
76.473 ± 0.007°
Cell volume
3763 ± 3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.179
Residual factor for significantly intense reflections
0.095
Weighted residual factors for significantly intense reflections
0.245
Weighted residual factors for all reflections included in the refinement
0.288
Goodness-of-fit parameter for all reflections included in the refinement
