Information card for entry 7104120

Structure parameters

• Formula: C22 H34 Cl P Pd Si2
• Calculated formula: C22 H34 Cl P Pd Si2
• Title of publication: 1-phosphabarrelene complexes of palladium and their use in Suzuki-Miyaura coupling reactions.
• Authors of publication: Blug, Matthias; Guibert, Clément; Le Goff, Xavier-Frederic; Mézailles, Nicolas; Le Floch, Pascal
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal volume: 34
• Journal issue: 2
• Pages of publication: 201 - 203
• a: 10.056 ± 0.001 Å
• b: 15.49 ± 0.001 Å
• c: 16.211 ± 0.001 Å
• α: 86.602 ± 0.001°
• β: 83.472 ± 0.001°
• γ: 89.719 ± 0.001°
• Cell volume: 2504.4 ± 0.3 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0723
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1369
• Weighted residual factors for all reflections included in the refinement: 0.1479
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No