Information card for entry 7104133

Structure parameters

• Formula: C8 H253 As10 Cs15.31 Na15.69 O436 W88 Yb10
• Calculated formula: C8 As10 Cs15.31 Na15.69 O436 W88 Yb10
• Title of publication: Polyoxotungstate-encapsulated Gd(6) and Yb(10) complexes.
• Authors of publication: Hussain, Firasat; Gable, Robert W; Speldrich, Manfred; Kögerler, Paul; Boskovic, Colette
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 328 - 330
• a: 21.476 ± 0.003 Å
• b: 24.164 ± 0.003 Å
• c: 27.725 ± 0.004 Å
• α: 70.632 ± 0.002°
• β: 70.009 ± 0.002°
• γ: 76.675 ± 0.003°
• Cell volume: 12644 ± 3 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1483
• Residual factor for significantly intense reflections: 0.0938
• Weighted residual factors for significantly intense reflections: 0.2223
• Weighted residual factors for all reflections included in the refinement: 0.2536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No