Information card for entry 7104153

Structure parameters

• Formula: C108 H144 As3 N6
• Calculated formula: C107 H130 As3 N6
• Title of publication: beta-Diiminato complexes of arsenic including the formally AsI compound [As3L3] [L = [N(C6H3Pri2-2,6)C(H)]2CPh].
• Authors of publication: Hitchcock, Peter B; Lappert, Michael F; Li, Gang; Protchenko, Andrey V
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 4
• Pages of publication: 428 - 429
• a: 15.5396 ± 0.0004 Å
• b: 18.7915 ± 0.0004 Å
• c: 19.6985 ± 0.0005 Å
• α: 101.334 ± 0.002°
• β: 96.248 ± 0.001°
• γ: 110.643 ± 0.002°
• Cell volume: 5177.5 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1376
• Residual factor for significantly intense reflections: 0.0882
• Weighted residual factors for significantly intense reflections: 0.2041
• Weighted residual factors for all reflections included in the refinement: 0.2259
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No