Information card for entry 7104188

Structure parameters

• Formula: C38 H36 Cl4 P2 Zn
• Calculated formula: C38 H35.94 Cl4 P2 Zn
• Title of publication: Facile dichloromethane activation and phosphine methylation. Isolation of unprecedented zwitterionic organozinc and organocobalt intermediates.
• Authors of publication: Pattacini, Roberto; Jie, Suyun; Braunstein, Pierre
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 8
• Pages of publication: 890 - 892
• a: 15.4168 ± 0.0006 Å
• b: 15.4168 ± 0.0006 Å
• c: 15.4168 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3664.4 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 198
• Hermann-Mauguin space group symbol: P 21 3
• Hall space group symbol: P 2ac 2ab 3
• Residual factor for all reflections: 0.0808
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.0815
• Weighted residual factors for all reflections included in the refinement: 0.0924
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No