Information card for entry 7104195

Structure parameters

• Formula: C38 H36 Cl6 P2 Zn2
• Calculated formula: C38 H36 Cl6 P2 Zn2
• Title of publication: Facile dichloromethane activation and phosphine methylation. Isolation of unprecedented zwitterionic organozinc and organocobalt intermediates.
• Authors of publication: Pattacini, Roberto; Jie, Suyun; Braunstein, Pierre
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 8
• Pages of publication: 890 - 892
• a: 10.0538 ± 0.0003 Å
• b: 13.6096 ± 0.0004 Å
• c: 15.0143 ± 0.0004 Å
• α: 91.832 ± 0.002°
• β: 102.291 ± 0.002°
• γ: 98.875 ± 0.002°
• Cell volume: 1978.84 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.061
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0938
• Weighted residual factors for all reflections included in the refinement: 0.1174
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No