Information card for entry 7104306

Structure parameters

• Formula: C176 H176 Ag8 N24 O52 S8
• Calculated formula: C176 H138 Ag8 N24 O52 S8
• Title of publication: 1D Infinite silver(i) chains reside in the big cavities built by the novel p-sulfonatocalix[4]arene-trisilver blocks.
• Authors of publication: Xiong, Kecai; Wu, Mingyan; Zhang, Qingfu; Wei, Wei; Yang, Ming; Jiang, Feilong; Hong, Maochun
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 14
• Pages of publication: 1840 - 1842
• a: 14.323 ± 0.002 Å
• b: 14.516 ± 0.002 Å
• c: 22.911 ± 0.003 Å
• α: 76.552 ± 0.004°
• β: 79.765 ± 0.004°
• γ: 89.185 ± 0.005°
• Cell volume: 4557.3 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0727
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for significantly intense reflections: 0.1932
• Weighted residual factors for all reflections included in the refinement: 0.2094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No