Information card for entry 7104528

Structure parameters

• Formula: C73 H61 F3 O5 P4 Pt2 S3
• Calculated formula: C73 H61 F3 O5 P4 Pt2 S3
• Title of publication: One-pot oxidation and protonation of a bridging sulfide and rare crystallographic evidence of a coordinated [SO] complex in [Pt2(micro-S2O2H)(PPh3)4]+.
• Authors of publication: Li, Jingqiu; Koh, Lip Lin; Hor, T S Andy
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 23
• Pages of publication: 3416 - 3418
• a: 18.2167 ± 0.0008 Å
• b: 10.3392 ± 0.0004 Å
• c: 18.3226 ± 0.0008 Å
• α: 90°
• β: 107.462 ± 0.001°
• γ: 90°
• Cell volume: 3292 ± 0.2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0285
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0619
• Weighted residual factors for all reflections included in the refinement: 0.0637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No