Information card for entry 7104693

Structure parameters

• Common name: trans-3,13-di(3-azidopropyl)-3,13-dimethyl- 1,5,7,9,11,15,17,19- octaphenylhexacyclo(15.3.1(1,13).1(3,11).1(5,17).1(9,15))decasiloxane
• Formula: C56 H58 N6 O14 Si10
• Calculated formula: C56 H58 N6 O14 Si10
• Title of publication: Synthesis and characterization of highly pure azido-functionalized polyhedral oligomeric silsesquioxanes (POSS)
• Authors of publication: Vuthichai Ervithayasuporn; Xin Wang; Yusuke Kawakami
• Journal of publication: Chem. Commun.
• Year of publication: 2009
• Journal volume: 34
• Pages of publication: 5130 - 5132
• a: 9.9231 ± 0.0002 Å
• b: 13.2854 ± 0.0003 Å
• c: 13.9868 ± 0.0007 Å
• α: 68.252 ± 0.0013°
• β: 71.0568 ± 0.0013°
• γ: 68.8461 ± 0.0013°
• Cell volume: 1557.98 ± 0.09 ų
• Cell temperature: 93.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0662
• Weighted residual factors for all reflections included in the refinement: 0.1652
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No