Information card for entry 7104720

Structure parameters

• Formula: C17 H30 B10 Cl2 N2 Sn
• Calculated formula: C17 H30 B10 Cl2 N2 Sn
• Title of publication: Exopolyhedral ligand flipping on isomerisation of novel supraicosahedral stannacarboranes.
• Authors of publication: Abram, Peter D; Ellis, David; Rosair, Georgina M; Welch, Alan J
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 36
• Pages of publication: 5403 - 5405
• a: 12.0192 ± 0.0015 Å
• b: 17.184 ± 0.002 Å
• c: 12.2211 ± 0.0015 Å
• α: 90°
• β: 99.762 ± 0.004°
• γ: 90°
• Cell volume: 2487.5 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0675
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1167
• Weighted residual factors for all reflections included in the refinement: 0.1248
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No