Information card for entry 7104722
| Formula |
C29 H32 Cl2 N6 O9 Zn4 |
| Calculated formula |
C28.999 H31.998 Cl1.998 N6 O9 Zn4 |
| Title of publication |
A novel Kolbe reaction pathway for a selective one- and two-electron reduction of azo compounds. |
| Authors of publication |
Fu, Wen-Fu; Li, Huifang-Jie; Wang, De-Hui; Zhou, Liang-Jun; Li, Li; Gan, Xin; Xu, Quan-Qing; Song, Hai-Bin |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2009 |
| Journal volume |
34 |
| Journal issue |
37 |
| Pages of publication |
5524 - 5526 |
| a |
22.926 ± 0.003 Å |
| b |
12.283 ± 0.0017 Å |
| c |
26.975 ± 0.003 Å |
| α |
90° |
| β |
104.015 ± 0.002° |
| γ |
90° |
| Cell volume |
7370 ± 1.5 Å3 |
| Cell temperature |
298 ± 2 K |
| Ambient diffraction temperature |
298 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
15 |
| Hermann-Mauguin space group symbol |
C 1 2/c 1 |
| Hall space group symbol |
-C 2yc |
| Residual factor for all reflections |
0.1217 |
| Residual factor for significantly intense reflections |
0.0526 |
| Weighted residual factors for significantly intense reflections |
0.0967 |
| Weighted residual factors for all reflections included in the refinement |
0.1138 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.886 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7104722.html
