Information card for entry 7104928

Structure parameters

• Formula: C6 F12 N2 O2 S4 Sb2
• Calculated formula: C6 F12 N2 O2 S4 Sb2
• Title of publication: The preparation of the MF6- (M = As, Sb) salts of 1,4-benzoquinodal bridged bis-1,3,2-dithiazolylium utilizing the cycloaddition and oxidative dehydrogenation chemistry of SNSMF6 and observation of a hybrid semiquinoidal-thiazyl radical-cation by EPR.
• Authors of publication: Decken, Andreas; Mailman, Aaron; Passmore, Jack
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 40
• Pages of publication: 6077 - 6079
• a: 6.7574 ± 0.0012 Å
• b: 7.6967 ± 0.0014 Å
• c: 17.669 ± 0.003 Å
• α: 87.882 ± 0.002°
• β: 88.198 ± 0.002°
• γ: 70.539 ± 0.002°
• Cell volume: 865.7 ± 0.3 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.027
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0684
• Weighted residual factors for all reflections included in the refinement: 0.069
• Goodness-of-fit parameter for all reflections included in the refinement: 1.19
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No