Information card for entry 7104930

Structure parameters

• Formula: C34 H41 N8 Ni2 O0.5
• Calculated formula: C34 H41 N8 Ni2 O0.5
• Title of publication: Redox-noninnocence of N,N'-bis(6-methyl-2-pyridylmethylene)ethane-1,2-diamine (L): synthesis and characterization of diamagnetic [Ni(II)2(L**)2] and [Zn(II)2(L)Cl4]((L**)2- pi diradical dianion of L).
• Authors of publication: Mondal, Amrita; Weyhermüller, Thomas; Wieghardt, Karl
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 40
• Pages of publication: 6098 - 6100
• a: 17.529 ± 0.002 Å
• b: 8.8499 ± 0.0009 Å
• c: 20.938 ± 0.002 Å
• α: 90°
• β: 97.06 ± 0.002°
• γ: 90°
• Cell volume: 3223.5 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0365
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0791
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No