Information card for entry 7105043

Structure parameters

• Common name: ((DIPP-nacnac)MgBH4)2
• Formula: C58 H90 B2 Mg2 N4
• Calculated formula: C58 H90 B2 Mg2 N4
• Title of publication: Synthesis and structure of a magnesium-amidoborane complex and its role in catalytic formation of a new bis-aminoborane ligand.
• Authors of publication: Spielmann, Jan; Bolte, Michael; Harder, Sjoerd
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 45
• Pages of publication: 6934 - 6936
• a: 14.3266 ± 0.0011 Å
• b: 13.9025 ± 0.0008 Å
• c: 15.1584 ± 0.0013 Å
• α: 90°
• β: 106.287 ± 0.006°
• γ: 90°
• Cell volume: 2898 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.1238
• Weighted residual factors for all reflections included in the refinement: 0.1298
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No