Information card for entry 7105064

Structure parameters

• Formula: C16 H64 La2 N16 Se8 Sn2
• Calculated formula: C15.8 H63.6 La2 N16 Se8 Sn2
• Title of publication: An unprecedented mu4-Sn2Se9 ligand: solvothermal syntheses and characterizations of novel lanthanum selenidostannates [{La(dien)2}4(mu4-Sn2Se9)(mu-Sn2Se6)]infinity and [La2(en)8(mu-Se2)]Sn2Se6.
• Authors of publication: Chen, Jiang-Fang; Jin, Qin-Yan; Pan, Ying-Li; Zhang, Yong; Jia, Ding-Xian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 46
• Pages of publication: 7212 - 7214
• a: 10.079 ± 0.0016 Å
• b: 14.843 ± 0.002 Å
• c: 14.918 ± 0.002 Å
• α: 90°
• β: 90.599 ± 0.004°
• γ: 90°
• Cell volume: 2231.7 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.1103
• Weighted residual factors for all reflections included in the refinement: 0.126
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No